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9701 · 33.3

Acyl chlorides flashcards

Revision flashcards for Cambridge 9701 Acyl chlorides (syllabus 33.3). Flip, recall, then mark a real past-paper question.

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    What is the functional group of an acyl chloride?

    The -COCl group, known as the acyl chloride or acid chloride group.

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    How are acyl chlorides named?

    Replace the '-oic acid' from the parent carboxylic acid with '-oyl chloride'. For example, ethanoic acid becomes ethanoyl chloride.

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    Name a reagent used to convert a carboxylic acid into an acyl chloride.

    Thionyl chloride ($SOCl_2$) or phosphorus(V) chloride ($PCl_5$).

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    Write the balanced equation for the reaction of ethanoic acid with thionyl chloride.

    $CH_3COOH + SOCl_2 \rightarrow CH_3COCl + SO_2(g) + HCl(g)$

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    Why is thionyl chloride ($SOCl_2$) often the preferred reagent for synthesising acyl chlorides in the lab?

    Because its by-products, sulfur dioxide ($SO_2$) and hydrogen chloride (HCl), are gases, which are easily removed from the liquid product, simplifying purification.

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    What is observed when ethanoyl chloride reacts with water?

    A vigorous/violent reaction occurs, producing steamy white fumes of hydrogen chloride (HCl) and aqueous ethanoic acid.

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    What type of mechanism do acyl chlorides undergo in their characteristic reactions?

    Nucleophilic addition-elimination.

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    What are the products of the reaction between propanoyl chloride and ethanol?

    Ethyl propanoate (an ester) and hydrogen chloride. $CH_3CH_2COCl + CH_3CH_2OH \rightarrow CH_3CH_2COOCH_2CH_3 + HCl$.

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    Why is the reaction of an acyl chloride with an alcohol a better method for esterification than using a carboxylic acid?

    The reaction is much faster, occurs at room temperature, and is irreversible (goes to completion), leading to a higher yield.

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    What are the products when butanoyl chloride reacts with excess ammonia?

    Butanamide ($CH_3CH_2CH_2CONH_2$) and ammonium chloride ($NH_4Cl$). Two moles of ammonia are required per mole of acyl chloride.

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    What is the product of the reaction between ethanoyl chloride and methylamine ($CH_3NH_2$)?

    An N-substituted amide, N-methylethanamide ($CH_3CONHCH_3$), and methylammonium chloride ($CH_3NH_3Cl$).

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    Why are acyl chlorides so much more reactive than esters?

    The chloride ion ($Cl^−$) is an excellent leaving group as it is the conjugate base of a strong acid (HCl). The ethoxide ion ($CH_3CH_2O^−$) from an ester is a poor leaving group as it is the conjugate base of a weak acid (ethanol).